Mt. Hood Community College Annotating 1 HNmr Spectrum and C 13 Nmr Spectra of Stilbene Oxide Project
Hi,
I need help annotating 1 H NMR spectra and C
–
13 spectra of stilbene oxide. If you could please label on the actual spectra’s, that’d be greatly appreciated.
Here are further instructions for annotating the NMR and 13C NMRs spectrum
1.
Draw the structure of stilbene oxide on the NMR spectrum printout
2.
For each signal
A. Label it with a formula or letter that matches the structure that you drew in the previous step. The goal is to
indicate which Hs (or Cs, for
C-13 NMR)
cause each signal.
B. Describe its multiplicity (singlet, doublet, triplet, doublet of doublets, multiplet
, etc.)
0.071
0.011
-0.000
-0.011
1.547
3.869
7.385
7.381
7.367
7.358
7.345
7.333
7.254
Current Data Parameters
NAME
S_Carpenter
EXPNO
10
PROCNO
1
F2 – Acquisition Parameters
Date_
20230201
Time
13.30 h
INSTRUM
spect
PROBHD
Z104275_0210 (
PULPROG
zg30
TD
65536
SOLVENT
CDCl3
NS
16
DS
2
SWH
6009.615 Hz
FIDRES
0.183399 Hz
AQ
5.4525952 sec
RG
188.16
DW
83.200 usec
DE
13.51 usec
TE
294.8 K
D1
1.00000000 sec
TD0
1
SFO1
300.1318533 MHz
NUC1
1H
P0
4.04 usec
P1
12.12 usec
PLW1
11.22000027 W
F2 – Processing parameters
SI
65536
SF
300.1300092 MHz
WDW
EM
SSB
0
LB
0.30 Hz
GB
0
PC
1.00
7.0
6.5
6.0
5.5
5.0
4.5
4.0
1.00
7.5
5.08
8.0
3.5
3.0
2.5
2.0
1.5
1.0
0.5
ppm